Qualitative and quantitative HPLC-ELSD-ESI-MS analysis of steroidal saponins in fenugreek seed
作者: Barbara Król-KogusDaniel GłódMirosława Krauze-Baranowska
作者单位: 1Department of Pharmacognosy with Medicinal Plants Garden , Medical University of Gdańsk , 80-416 Gdańsk , Poland
刊名: Acta Pharmaceutica, 2020, Vol.70 (1), pp.89-99
来源数据库: De Gruyter Journal
DOI: 10.2478/acph-2020-0013
关键词: Fenugreek seedsSaponinsHPLC-ELSD-ESI-MSQualitative and quantitative analysis
原始语种摘要: Abstract Fenugreek seeds are known as a source of various compounds, the most common of which are steroidal saponins. However, despite the growing interest in this plant material as a healing agent, spice and dietary supplement ingredient, the composition of Polish fenugreek seeds remains unknown. Therefore, the steroidal saponin complex in the seeds of T. foenum-graecum cultivated in Poland was qualitatively and quantitatively analyzed by the HPLC-ELSDESI-MS method. Two C-18 columns connected in series were used for the first time in analysis of fenugreek saponins and ELS detector parameters were optimized. A total of 26 furostanol saponins were revealed, of which 24 were tentatively identified. The HPLC-ELSD method developed for quantitative analysis was preliminarily validated and the...
全文获取路径: De Gruyter 

  • 从质量方面看 不知道的
  • saponins 皂甙
  • fenugreek 胡芦巴
  • steroidal 甾族的
  • quantitative 量的
  • analysis 分析
  • remains 残渣
  • unknown 不知道的
  • qualitatively 不知道的
  • cultivated 栽培的
  • healing 加硫