Simultaneous and Rapid Determination of Main Lignans in Different Parts of Schisandra Sphenanthera by Micellar Electrokinetic Capillary Chromatography
作者: Guangxin YuanYang LiuTan LiYan WangYu ShengMing Guan
刊名: Molecules, 2011, Vol.16 (5), pp.3713
来源数据库: Directory of Open Access Journals
关键词: micellar electrokinetic capillary chromatography (MEKC)lignansdifferent plant partsSchisandra sphenanthera
原始语种摘要: Lignans are imporant active ingredients of Schisandra sphenanthera. A micellar electrokinetic chromatography method was developed for the simultaneous determination of eight lignans – schizandrin, schisandrol B, schisantherin A, schisanhenol, anwulignan, deoxyschizandrin, schizandrin B and schizandrin C – in different parts of S. sphenanthera. The key factors for separation and determination were studied and the best analysis conditions were obtained using a background electrolyte of 10 mM phosphate-37.5 mM SDS-35% v/v acetonitrile (pH 8.0) at the separation voltage of 28 kV and detection at 214 nm, whereby the plant samples could be analyzed within 9.0 min. Analysis yielded good reproducibility (RSD between 1.19-2.28%) and good recovery (between 92.2-103.8%). The detection limits (LOD)...
全文获取路径: DOAJ  (合作)
影响因子:2.428 (2012)

  • Schisandra 五味子
  • schizandrin 五味子素
  • lignans 木脂素类
  • determination 测定
  • phosphate 磷酸盐
  • electrokinetic 动电学
  • acetonitrile 乙腈
  • within 在以内
  • whereby 借此
  • SDS Satellite Data System