4‐Methyl‐ N ‐[2‐( p ‐tolylsulfanyl)phenyl]benzene­sulfonamide
作者: Surajit BanerjeeAlok K. MukherjeeBidisha NandiNitya G. KunduMadeleine Helliwell
作者单位: 1Department of Physics, Jadavpur University, Calcutta 700 032, India
2 Department of Organic Chemistry, Indian Association for the Cultivation of Science, Jadavpur, Calcutta 700 032, India
3 Department of Chemistry, University of Manchester, Manchester M13 9PL, England
刊名: Acta Crystallographica Section C, 2000, Vol.56 (12), pp.1490-1491
来源数据库: Wiley Journal
DOI: 10.1107/S0108270100012725
原始语种摘要: The title compound, C20H19NO2S2, is formed by a palladium–copper‐catalyzed reaction between 4‐methyl‐ N ‐[2‐(prop‐2‐ynyl­sul­fanyl)­phenyl]­benzene­sul­fon­amide and p ‐iodo­toluene. The mol­ecules contain three essentially planar parts, namely an amino­thio­phenol moiety ( A ), a toluene­sulfone moiety excluding the oxo ligands ( B ) and a tolyl group ( C ), approximately orthogonal to each other; the dihedral angles A / B , A / C and B / C are 111.6 (1), 89.3 (1) and 101.4 (1)°, respectively. Intermolecular N—H⃛O hydrogen bonds link the mol­ecules into infinite one‐dimensional chains.
全文获取路径: Wiley  (合作)

  • phenyl 苯基
  • sulfonamide 磺酰胺
  • benzene 
  • moiety 一部分
  • dihedral 二面角
  • toluene 甲苯
  • palladium 
  • reaction 反酌
  • essentially 本质上
  • sulfone