Quantification of Piperazine in Chicken Muscle by Ultra-Performance Liquid Chromatography-Electrospray Ionization Tandem Mass Spectrometry
作者: Kaizhou XieYa’nan LiuLirui SunMaoda PangXing XieQiang GaoBo WangYangyang ZhangRan WangGenxi ZhangGuojun DaiJinyu Wang
作者单位: 1Yangzhou University
2Key Laboratory for Animal Genetic, Breeding, Reproduction and Molecular Design of Jiangsu Province
3Jiangsu Academy of Agricultural Sciences
4Key Laboratory for Animal
刊名: Food Analytical Methods, 2017, Vol.10 (6), pp.1736-1744
来源数据库: Springer Journal
DOI: 10.1007/s12161-016-0717-x
关键词: PiperazineUPLC-ESI/MS/MSChicken muscle
英文摘要: An ultra-performance liquid chromatography-electrospray ionization tandem triple quadrupole mass spectrometry (UPLC-ESI/MS/MS) method was developed for the detection of piperazine in chicken muscle. Following extraction and purification, the chicken muscle extract was injected into the UPLC system and analyzed. Piperazine detection was performed on a triple-quadrupole mass spectrometer with the ESI interface operating in positive mode. The most sensitive mass transition from the precursor ion to the product ion was 87.1 → 44.1 for piperazine. The coefficient ( R 2) of piperazine was 0.9995 in the range of 1–200 μg/kg. The recovery and relative standard deviation (RSD) ranged from 102.93 to 111.46% and from 4.57 to 5.28% at 50.0, 100.0 and 200.0 μg/kg adding levels,...
原始语种摘要: An ultra-performance liquid chromatography-electrospray ionization tandem triple quadrupole mass spectrometry (UPLC-ESI/MS/MS) method was developed for the detection of piperazine in chicken muscle. Following extraction and purification, the chicken muscle extract was injected into the UPLC system and analyzed. Piperazine detection was performed on a triple-quadrupole mass spectrometer with the ESI interface operating in positive mode. The most sensitive mass transition from the precursor ion to the product ion was 87.1 → 44.1 for piperazine. The coefficient ( R 2) of piperazine was 0.9995 in the range of 1–200 μg/kg. The recovery and relative standard deviation (RSD) ranged from 102.93 to 111.46% and from 4.57 to 5.28% at 50.0, 100.0 and 200.0 μg/kg adding levels,...
全文获取路径: Springer  (合作)
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影响因子:1.969 (2012)

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关键词翻译
关键词翻译
  • 四极透镜 量化
  • piperazine 哌嗪
  • muscle 肌肉
  • tandem 串联机
  • ionization 电离化
  • derivative 衍生物
  • extraction 提取
  • detection 探测
  • chicken 小鸡
  • quantification 量化
  • quadrupole 量化