Accurate Determination of Tributyltin in Tannery Wastewater by a New Procedure Using ID-HPLC–ICP-MS Combined with Low Temperature Extraction
作者: Yang ZhaoZhiding HuangChao WeiQian WangKe XieWenkai ChangChunhua WuYong WangXiaoxia QiZenghe Li
作者单位: 1National Footwear Quality Supervision and Inspection Center (Beijing), China Leather and Footwear Industry Research Institute
2Beijing University of Chemical Technology
3National Institute of Metrology, China
4Agilent Technologies
刊名: Chromatographia, 2017, Vol.80 (11), pp.1623-1631
来源数据库: Springer Journal
DOI: 10.1007/s10337-017-3394-z
关键词: HPLC–ICP-MSIsotope dilutionLow temperature extractionTributyltinTannery wastewater
英文摘要: Isotope dilution mass spectrometry is recognized as a primary method to obtain traceable values in the measurement of substances including trace elements and their organometallic compounds. This paper reports a novel method where isotope dilution high performance liquid chromatography inductively coupled plasma mass spectrometry (ID-HPLC–ICP-MS) was combined with low temperature extraction for the determination of tributyltin (TBT) in tannery wastewater from the leather industry. It has been found that the liquid–liquid extraction at very low temperature is in the favor of extraction of organotin, as the enrichment factor for low temperature (−80 °C) extraction was about 1.3 times higher than for extraction at room temperature (20 °C). The method detection limit of TBT, obtained from the...
原始语种摘要: Isotope dilution mass spectrometry is recognized as a primary method to obtain traceable values in the measurement of substances including trace elements and their organometallic compounds. This paper reports a novel method where isotope dilution high performance liquid chromatography inductively coupled plasma mass spectrometry (ID-HPLC–ICP-MS) was combined with low temperature extraction for the determination of tributyltin (TBT) in tannery wastewater from the leather industry. It has been found that the liquid–liquid extraction at very low temperature is in the favor of extraction of organotin, as the enrichment factor for low temperature (−80 °C) extraction was about 1.3 times higher than for extraction at room temperature (20 °C). The method detection limit of TBT, obtained from the...
全文获取路径: Springer  (合作)
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影响因子:1.437 (2012)

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关键词翻译
关键词翻译
  • wastewater 废水
  • tannery 鞣革厂
  • tanning 
  • extraction 提取
  • range 射程
  • trace 痕迹
  • temperature 温度
  • dilution 稀度
  • values 价值观
  • higher